C₂₄H₂₄Cl₂N₂O₃

Base Information

Chemical Name:C₂₄H₂₄Cl₂N₂O₃
CAS No.:1191248-63-1
Molecular Formula:C₂₄H₂₄Cl₂N₂O₃
Molecular Weight:459.372
Hs Code.:

C<sub>24</sub>H<sub>24</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₄H₂₄Cl₂N₂O₃

Chemical Property:

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Technology Process of C₂₄H₂₄Cl₂N₂O₃

There total 9 articles about C₂₄H₂₄Cl₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5223-06-3
5-ethyl-2-(2-hydroxyethyl)pyridine

: 1173794-90-5
C₁₅H₁₃Cl₂NO₃

: 1191248-63-1
C₂₄H₂₄Cl₂N₂O₃

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In diethyl ether; at 20 ℃;
DOI:10.1016/j.cclet.2010.11.008

Reference yield:

: 1173794-83-6
C₁₅H₁₂Cl₃NO₂

: 1191248-63-1
C₂₄H₂₄Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / 2.5 h / 160 - 250 °C / Inert atmosphere

2: water; sodium hydroxide / 2 h / Reflux

3: toluene-4-sulfonic acid / 3 h / 80 °C

4: triphenylphosphine; diethylazodicarboxylate / diethyl ether / 20 °C

With aluminum (III) chloride; water; toluene-4-sulfonic acid; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In diethyl ether; 4: Mitsunobu reaction;
DOI:10.1016/j.cclet.2010.11.008

Reference yield:

: 1173794-86-9
C₁₄H₉Cl₂NO₂

: 1191248-63-1
C₂₄H₂₄Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / 2 h / Reflux

2: toluene-4-sulfonic acid / 3 h / 80 °C

3: triphenylphosphine; diethylazodicarboxylate / diethyl ether / 20 °C

With water; toluene-4-sulfonic acid; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In diethyl ether; 3: Mitsunobu reaction;
DOI:10.1016/j.cclet.2010.11.008