((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆

Base Information

Chemical Name:((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆
CAS No.:1005343-95-2
Molecular Formula:C₃₄H₄₀P₂Pd
Molecular Weight:617.059
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)PdC<sub>8</sub>H<sub>16</sub>

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Chemical Property of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆

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Technology Process of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆

There total 3 articles about ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 19978-61-1
(1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II)

: 45037-87-4
1,8-octanediyldimagnesium dibromide

: 1005343-95-2
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆

Guidance literature:: In not given;
DOI:10.1016/j.jorganchem.2007.10.025

Reference yield: 11.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 45037-87-4
1,8-octanediyldimagnesium dibromide

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 1005343-95-2
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆

Guidance literature:: In tetrahydrofuran; under N2 atm. soln. BrMg(CH2)8MgBr in THF was added to suspn. PdCl2(COD)in Et2O at -78°C, stirred for 30 min, warmed to r.t., stirred fo r 30 min, pentane was added, supernatant was evapd. in vacuo, dissolved in Et2O, dppe was added, 30 min; ppt. was washed with Et2O and dried in vacuo for 30 min;
DOI:10.1016/j.jorganchem.2007.10.025

Reference yield:

: ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₄

: 1333-74-0
hydrogen

: 1005343-95-2
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)PdC₈H₁₆

Guidance literature:: With palladium on activated charcoal; In diethyl ether; Pd/C was added to soln. Pd complex in Et2O and stirred under H2 atm. (1 atm.) for 46 h; react. mixt. was filtered, solvent was removed in vacuo;
DOI:10.1016/j.jorganchem.2007.10.025