C₃₀H₁₆F₁₂N₂C₁₆H₃₆N⁽¹⁺⁾C₂H₃O₂^(1-)

Base Information

Chemical Name:C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-)
CAS No.:1619919-88-8
Molecular Formula:C₂H₃O₂*C₁₆H₃₆N*C₃₀H₁₆F₁₂N₂
Molecular Weight:933.964
Hs Code.:

C<sub>30</sub>H<sub>16</sub>F<sub>12</sub>N<sub>2</sub>*C<sub>16</sub>H<sub>36</sub>N<sup>(1+)</sup>*C<sub>2</sub>H<sub>3</sub>O<sub>2</sub><sup>(1-)</sup>

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Chemical Property of C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-)

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Technology Process of C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-)

There total 4 articles about C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 626-19-7
Isophthalaldehyde

: 1619919-88-8
C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron trifluoride diethyl etherate / toluene / 150 °C / Inert atmosphere; Dean-Stark

2.1: zinc / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; piperidine / N,N-dimethyl-formamide / 24 h / 80 °C / Schlenk technique; Inert atmosphere

4.1: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 48 h / 80 °C / Schlenk technique; Inert atmosphere

5.1: acetonitrile / 24.84 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; zinc; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: |Barbier Coupling Reaction / 2.2: |Barbier Coupling Reaction / 3.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c4ob00357h

Reference yield:

: 1619919-70-8
N,N'-(1,3-phenylenebis(but-3-yne-1,1-diyl))bis(4-methylbenzenesulfonamide)

: 1619919-88-8
C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; piperidine / N,N-dimethyl-formamide / 24 h / 80 °C / Schlenk technique; Inert atmosphere

2: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 48 h / 80 °C / Schlenk technique; Inert atmosphere

3: acetonitrile / 24.84 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1039/c4ob00357h

Reference yield:

: 1619919-72-0
N,N'-(1,3-phenylenebis(4-(3,5-bis(trifluoromethyl)phenyl)but-3-yne-1,1-diyl))bis(4-methylbenzenesulfonamide)

: 1619919-88-8
C₃₀H₁₆F₁₂N₂*C₁₆H₃₆N⁽¹⁺⁾*C₂H₃O₂^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 48 h / 80 °C / Schlenk technique; Inert atmosphere

2: acetonitrile / 24.84 °C

With tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c4ob00357h