C₁₂H₁₄N₄O

Base Information

Chemical Name:C₁₂H₁₄N₄O
CAS No.:1404065-21-9
Molecular Formula:C₁₂H₁₄N₄O
Molecular Weight:230.269
Hs Code.:

C<sub>12</sub>H<sub>14</sub>N<sub>4</sub>O

Synonyms:

Suppliers and Price of C₁₂H₁₄N₄O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₄N₄O

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₂H₁₄N₄O

There total 6 articles about C₁₂H₁₄N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-76-2
levulinic acid

: 1404065-21-9
C₁₂H₁₄N₄O

Guidance literature:: Multi-step reaction with 7 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: bromine; acetic acid / 6 h / 90 °C

3: hydrazine hydrate / 16 h / 150 - 160 °C

4: nitric acid; sulfuric acid / 3 h / 0 - 20 °C

5: sulfuric acid / 5 h / 55 - 60 °C

6: potassium carbonate / N,N-dimethyl-formamide / 16 h / 110 °C

7: acetic acid; iron / 12 h / Reflux

With sulfuric acid; bromine; nitric acid; iron; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.07.077

Reference yield:

: 5157-08-4
3-methyl-4,5-dihydro-6-oxopyridazine

: 1404065-21-9
C₁₂H₁₄N₄O

Guidance literature:: Multi-step reaction with 6 steps

1: bromine; acetic acid / 6 h / 90 °C

2: hydrazine hydrate / 16 h / 150 - 160 °C

3: nitric acid; sulfuric acid / 3 h / 0 - 20 °C

4: sulfuric acid / 5 h / 55 - 60 °C

5: potassium carbonate / N,N-dimethyl-formamide / 16 h / 110 °C

6: acetic acid; iron / 12 h / Reflux

With sulfuric acid; bromine; nitric acid; iron; potassium carbonate; hydrazine hydrate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.07.077

Reference yield:

: 13327-27-0
6-Methylpyridazin-3(2H)-on

: 1404065-21-9
C₁₂H₁₄N₄O

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine hydrate / 16 h / 150 - 160 °C

2: nitric acid; sulfuric acid / 3 h / 0 - 20 °C

3: sulfuric acid / 5 h / 55 - 60 °C

4: potassium carbonate / N,N-dimethyl-formamide / 16 h / 110 °C

5: acetic acid; iron / 12 h / Reflux

With sulfuric acid; nitric acid; iron; potassium carbonate; hydrazine hydrate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.07.077