N--O-methylsulphonylhydroxylamine

Base Information

Chemical Name:N--O-methylsulphonylhydroxylamine
CAS No.:129529-00-6
Molecular Formula:C₁₇H₂₂NO₄PS
Molecular Weight:367.406
Hs Code.:

N-<bis(4-methylbenzyl)phosphinoyl>-O-methylsulphonylhydroxylamine

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Suppliers and Price of N--O-methylsulphonylhydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--O-methylsulphonylhydroxylamine

Chemical Property:

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Technology Process of N--O-methylsulphonylhydroxylamine

There total 5 articles about N--O-methylsulphonylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 129528-99-0
N-hydroxylamine

: 124-63-0
methanesulfonyl chloride

: 129529-00-6
N--O-methylsulphonylhydroxylamine

Guidance literature:: With pyridine; cooling;

Reference yield:

: 18896-84-9
bis(4-methylbenzyl)phosphinic acid

: 129529-00-6
N--O-methylsulphonylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / CH₂Cl₂ / 1 h

2: 1) O-trimethylsilylhydroxylamine, triethylamine, 2) methanol / 1) dichloromethane, 1h, room temp.

3: 39 percent / pyridine / cooling

With pyridine; methanol; oxalyl dichloride; O-Trimethylsilylhydroxylamine; triethylamine; In dichloromethane;

Reference yield:

: 129528-98-9
bis(4-methylbenzyl)phosphine oxide

: 129529-00-6
N--O-methylsulphonylhydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / 30percent hydrogen peroxide / methanol / 1.5 h / 90 °C

2: oxalyl chloride / CH₂Cl₂ / 1 h

3: 1) O-trimethylsilylhydroxylamine, triethylamine, 2) methanol / 1) dichloromethane, 1h, room temp.

4: 39 percent / pyridine / cooling

With pyridine; methanol; oxalyl dichloride; O-Trimethylsilylhydroxylamine; dihydrogen peroxide; triethylamine; In methanol; dichloromethane;