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triphenylarsine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

Base Information
  • Chemical Name:triphenylarsine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron
  • CAS No.:73979-11-0
  • Molecular Formula:C35H28AsFeNO2
  • Molecular Weight:625.381
  • Hs Code.:
triphenylarsine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

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Chemical Property of triphenylarsine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron
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Technology Process of triphenylarsine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

There total 2 articles about triphenylarsine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In toluene; at 60 - 80 °C,with 10 fold molar excess of AsPh3; recrystn. from non-polar solvent or sepn. by chromy. on Al2O3, eluent CH2Cl2/C6H14;
Guidance literature:
In toluene; 10 equiv. of AsPh3, deaerated solvent, 60°C, 24 h; chromy. (Al2O3, CH2Cl2/hexane), crystn. (CH2Cl2/hexane); elem. anal.;
DOI:10.1039/DT9770002181
Guidance literature:
Multi-step reaction with 2 steps
1: CO
2: benzene
With CO; In benzene;
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