6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene

Base Information

• Chemical Name: 6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene
• CAS No.: 84927-34-4
• Molecular Formula: C₂₀H₂₄N₄
• Molecular Weight: 320.437

Synonyms:

Chemical Property of 6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene

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Technology Process of 6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene

There total 1 articles about 6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

benzocyclohepta<1,4>oxazine (68521-38-0) + Trimethylenediamine (109-76-2,54018-94-9) → 2-phenyl-1,4,5,6-tetrahydropyrimidine (25099-77-8) + (6E,18E)-2,6,14,18-Tetraaza-tricyclo[17.5.0.07,13]tetracosa-1(24),6,8,10,12,18,20,22-octaene (84927-34-4)

Guidance literature:

In ethanol; Heating;

DOI:10.1039/a707825k

Reference yield: 94.0%

Hf(4+)*4CH2C6H5(1-)=[Hf(CH2C6H5)4] + 6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene (84927-34-4) → Hf(CH2C6H5)2(C7H5N2((CH2)3)2N2C7H5) (198290-80-1)

Guidance literature:

In pentane; inert atmosphere, absence of light; addn. of ligand to metal compd. at -30°C, stirring at 35°C for 1 h (pptn.); collection (filtration), washing (Et2O, pentane), drying; can be recrystallized by Et2O diffusion into CH2Cl2 soln. (several d);

Reference yield: 85.0%

tetrabenzylzirconium (24356-01-2) + 6,7,8,9,16,17,18,19-octahydrodicyclohepta[b,i][1,4,8,11]tetraazacyclotetradecene (84927-34-4) → Zr(CH2C6H5)2(C7H5N2((CH2)3)2N2C7H5) (198290-82-3)

Guidance literature:

In pentane; inert atmosphere, absence of light; addn. of ligand to metal compd. at -30°C, stirring at 35°C for 1 h (pptn.); collection (filtration), washing (Et2O, pentane), drying;

upstream raw materials:

benzocyclohepta<1,4>oxazine

Trimethylenediamine

Downstream raw materials:

Hf(CH₂C₆H₅)2(C₇H₅N₂((CH₂)3)2N₂C₇H₅)

Zr(CH₂C₆H₅)2(C₇H₅N₂((CH₂)3)2N₂C₇H₅)

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