5-(Benzyloxy)-2-bromonaphthalene-1,4-dione

Base Information

Chemical Name:5-(Benzyloxy)-2-bromonaphthalene-1,4-dione
CAS No.:119650-41-8
Molecular Formula:C17H11BrO3
Molecular Weight:343.177
Hs Code.:
DSSTox Substance ID:DTXSID70556403
Nikkaji Number:J2.912.268G
Wikidata:Q82437944
Mol file:119650-41-8.mol

Synonyms:119650-41-8;5-(Benzyloxy)-2-bromonaphthalene-1,4-dione;DTXSID70556403

Suppliers and Price of 5-(Benzyloxy)-2-bromonaphthalene-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 5-(Benzyloxy)-2-bromonaphthalene-1,4-dione

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:341.98916
Heavy Atom Count:21
Complexity:451

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=CC=CC3=C2C(=O)C=C(C3=O)Br

Technology Process of 5-(Benzyloxy)-2-bromonaphthalene-1,4-dione

There total 4 articles about 5-(Benzyloxy)-2-bromonaphthalene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 69008-03-3
2-bromo-5-hydroxy-[1,4]naphthoquinone

: 100-39-0
benzyl bromide

: 119650-41-8
5-(benzyloxy)-2-bromonaphthalene-1,4-dione

Guidance literature:: With silver(l) oxide; In dichloromethane; at 20 ℃; for 36h;
DOI:10.1002/anie.201005329

Reference yield: 61.0%

: 148914-36-7
5-Benzyloxy-2-bromo-naphthalen-1-ol

: 119650-41-8
5-(benzyloxy)-2-bromonaphthalene-1,4-dione

Guidance literature:: With [bis(acetoxy)iodo]benzene; water; In acetonitrile; at 0 - 23 ℃; for 0.333333h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.1c03530

Reference yield:

: 481-39-0
5-hydroxynaphtho-1,4-quinone

: 119650-41-8
5-(benzyloxy)-2-bromonaphthalene-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / Br₂; AcOH / CHCl₃ / 1.17 h / 0 °C

2: 84 percent / Ag₂O / CHCl₃ / 2 h

With bromine; acetic acid; silver(l) oxide; In chloroform;
DOI:10.1039/b102807n