Fe^III(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)₂

Base Information

• Chemical Name: Fe^III(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)₂
• CAS No.: 403519-72-2
• Molecular Formula: C₄₅H₂₈F₁₅FeN₄O₂
• Molecular Weight: 997.566
• Mol file: 403519-72-2.mol

Synonyms:

Chemical Property of Fe^III(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)₂

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Fe^III(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)₂

There total 1 articles about Fe^III(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

diethyl ether (60-29-7,927820-24-4) + iron(II) chloride + 5,10,15-tris(pentafluorophenyl)corrole → FeIII(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)2 (403519-72-2)

Guidance literature:

iron(II) chloride; 5,10,15-tris(pentafluorophenyl)corrole; In N,N-dimethyl-formamide; for 1h; Inert atmosphere; Reflux;

diethyl ether;

DOI:10.1016/j.ica.2016.07.007

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + FeIII(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)2 (403519-72-2) → 5,10,15-tris(pentafluorophenyl)corrole iron(IV) chloride (226922-75-4)

Guidance literature:

In dichloromethane; water;

DOI:10.1021/ic0491332

Reference yield:

FeIII(5,10,15-tripentafluorophenylcorrole trianion)(diethyl ether)2 (403519-72-2) + hydrogen bromide (10035-10-6,12258-64-9) → Fe(5,10,15-tris(pentafluorophenyl)corrole(3-))Br

Guidance literature:

In water; benzene;

DOI:10.1021/ic0491332

upstream raw materials:

diethyl ether

Downstream raw materials:

5,10,15-tris(pentafluorophenyl)corrole iron(IV) chloride