[(ferrocene-ethynyl)2PhPAuCl]

Base Information

Chemical Name:[(ferrocene-ethynyl)2PhPAuCl]
CAS No.:1144033-53-3
Molecular Formula:C₃₀H₂₃AuClFe₂P
Molecular Weight:758.6
Hs Code.:

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Chemical Property of [(ferrocene-ethynyl)2PhPAuCl]

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Technology Process of [(ferrocene-ethynyl)2PhPAuCl]

There total 1 articles about [(ferrocene-ethynyl)2PhPAuCl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 916074-57-2
di(ferrocenylethynyl)phenylphosphane

: 162718-91-4
ClAu(tetrahydrothiophene)

: 1144033-53-3
[(ferrocene-ethynyl)2PhPAuCl]

Guidance literature:: In tetrahydrofuran; (N2); using Schlenk techniques; addn. dropwise soln. of (ferrocene-ethynyl)2PhP (25% excess) to THF soln. containing of (THT)AuCl over a period of 1 h at 0°C; stirring at 25°C for 1 h; removal of all volatiles in vac., chromy. on silica gel with Et2O as eluent; elem. anal.;
DOI:10.1016/j.jorganchem.2008.11.046

Reference yield:

: 1271-47-2
ferroceneacetylene

: 1144033-53-3
[(ferrocene-ethynyl)2PhPAuCl]

: [(ferrocene-ethynyl)2PhPAu(ferrocene-ethynyl)]

Guidance literature:: copper(l) iodide; In diethylamine; (N2); using Schlenk techniques; treatment of diethylamine soln. of (ferrocene-ethynyl)2PhPAuCl with ethynylferrocene in the presence of (CuI); not separated;
DOI:10.1016/j.jorganchem.2008.11.046

Reference yield:

: (η(5)-C5H5)Ru(η(5)-C5H4CCH)

: 1144033-53-3
[(ferrocene-ethynyl)2PhPAuCl]

: [(ferrocene-ethynyl)2PhPAu(ruthenocene-ethynyl)]

Guidance literature:: copper(l) iodide; In diethylamine; (N2); using Schlenk techniques; treatment of diethylamine soln. of (ferrocene-ethynyl)2PhPAuCl with ethynyl ruthenocene in the presence of (CuI); not separated;
DOI:10.1016/j.jorganchem.2008.11.046