4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine

Base Information

Chemical Name:4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine
CAS No.:126440-70-8
Molecular Formula:C₁₈H₂₂N₂O₃S
Molecular Weight:346.45
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine

Chemical Property:

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Technology Process of 4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine

There total 7 articles about 4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 126411-72-1
4-tosyl-3,4,5,6-tetrahydro-2H-<1,4,7>benzoxadiazecine hydrochloride

: 126440-70-8
4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 2h; Heating;

Reference yield:

: 60633-78-5
2-(2-bromoethoxy)benzaldehyde

: 126440-70-8
4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / p-toluenesulfonic acid / benzene / 10 h / Heating

2: 1.) potassium tert-butanolate / 1.) DMF, 50 deg C, 2.) DMF, benzene, from 100 to 110 deg C, 15 h

3: 55 percent / aq. potassium hydroxide, methanol / 30 h / Heating

4: 58 percent / concd. hydrochloric acid / ethanol / 5 h / Heating

5: 23 percent / sodium borohydride / ethanol / 2 h / Heating

With hydrogenchloride; methanol; potassium hydroxide; sodium tetrahydroborate; potassium tert-butylate; toluene-4-sulfonic acid; In ethanol; benzene;

Reference yield:

: 3560-47-2
N-(2-((4-methylphenyl)sulfonamido)ethyl)acetamide

: 126440-70-8
4-tosyl-3,4,5,6,7,8-hexahydro-2H-<1,4,7>benzoxadiazecine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) potassium tert-butanolate / 1.) DMF, 50 deg C, 2.) DMF, benzene, from 100 to 110 deg C, 15 h

2: 55 percent / aq. potassium hydroxide, methanol / 30 h / Heating

3: 58 percent / concd. hydrochloric acid / ethanol / 5 h / Heating

4: 23 percent / sodium borohydride / ethanol / 2 h / Heating

With hydrogenchloride; methanol; potassium hydroxide; sodium tetrahydroborate; potassium tert-butylate; In ethanol;