(1Z,2Z)-benzil O,O-diacetyl dioxime

Base Information

Chemical Name:(1Z,2Z)-benzil O,O-diacetyl dioxime
CAS No.:134891-54-6
Molecular Formula:C₁₈H₁₆N₂O₄
Molecular Weight:324.336
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1Z,2Z)-benzil O,O-diacetyl dioxime

Chemical Property:

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Technology Process of (1Z,2Z)-benzil O,O-diacetyl dioxime

There total 11 articles about (1Z,2Z)-benzil O,O-diacetyl dioxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 572-45-2
benzil dioxime

: 108-24-7
acetic anhydride

: 17363-36-9,134891-54-6
(1Z,2Z)-benzil O,O-diacetyl dioxime

Guidance literature:: With pyridine; dmap; at 20 ℃; for 8h;
DOI:10.1021/acs.orglett.0c01260

Reference yield:

: 134-81-6
benzil

: 17363-36-9,134891-54-6
(1Z,2Z)-benzil O,O-diacetyl dioxime

Guidance literature:: Multi-step reaction with 2 steps

1: hydrochloric acid; methanol; hydroxylamine hydrochloride

With hydrogenchloride; methanol; hydroxylamine hydrochloride;

Reference yield:

: 13665-04-8
2,2-dibromoacetophenone

: 134891-54-6
benzil-bis-(O-acetyl-seqtrans-oxime )

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate; diluted alcohol; hydroxylamine hydrochloride / 70 - 80 °C

2: diluted NaOH-solution

3: sodium acetate

With sodium hydroxide; ethanol; hydroxylamine hydrochloride; sodium acetate;