Carbonimidic dichloride, (4-cyanophenyl)-

Base Information

• Chemical Name: Carbonimidic dichloride, (4-cyanophenyl)-
• CAS No.: 120672-82-4
• Molecular Formula: C8H4Cl2N2
• Molecular Weight: 199.039
• Mol file: 120672-82-4.mol

Synonyms:

Chemical Property of Carbonimidic dichloride, (4-cyanophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonimidic dichloride, (4-cyanophenyl)-

There total 1 articles about Carbonimidic dichloride, (4-cyanophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N-(4-cyanophenyl)formamide (6321-94-4) → p-cyanophenylcarbonimidoyl dichloride (120672-82-4)

Guidance literature:

With thionyl chloride; sulfuryl dichloride; for 24h; Heating;

DOI:10.1080/00397919208021105

Reference yield: 89.0%

p-cyanophenylcarbonimidoyl dichloride (120672-82-4) → 4-isocyanobenzonitrile (2980-80-5)

Guidance literature:

With lithium perchlorate; In N,N-dimethyl-formamide; at 15 ℃; Electrolysis;

DOI:10.1016/S0040-4020(99)00509-8

Reference yield: 73.0%

furil (492-94-4) + p-cyanophenylcarbonimidoyl dichloride (120672-82-4) → 2-(4-cyanophenylimino)-4,5-di(2-furyl)-1,3-dioxole (442199-54-4) + (E)-1,2-di(2-furyl)vinylene bis[N-(4-cyanophenyl)-chloroformimidate]

Guidance literature:

Inert atmosphere; Electrolysis;

DOI:10.1016/j.tet.2009.02.082

upstream raw materials:

N-(4-cyanophenyl)formamide

Downstream raw materials:

N-(4-Cyano-phenyl)-N',N''-dicyclooctyl-guanidine

N-(4-Cyano-phenyl)-N',N''-bis-(1H-tetrazol-5-ylmethyl)-guanidine

N-(4-cyanophenyl)-N'-cyclooctyl-N''-(1H-tetrazol-5-ylmethyl)guanidine

C₁₆H₁₄ClN₃

Refernces

• 1、 Nagarajan,Ho,DuBois. "A simple method for the synthesis of unsymmetrical trisubstituted guanidines". . p. 1191 - 1198. Retrieved 2007/10/02.