2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane

Base Information

Chemical Name:2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane
CAS No.:92831-90-8
Molecular Formula:C₂₈H₃₀O₁₀
Molecular Weight:526.54
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane

Chemical Property:

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Technology Process of 2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane

There total 2 articles about 2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3162-28-5
2-hydroxy-3,4,5,6-tetramethoxyacetophenone

: 92831-90-8
2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1. 1h, 50-60 deg C, 2. 2-3h, room temperature

2: 0.7 g / potassium hydroxide / pyridine / 1. 30 min, 45-50 deg C, 2. room temperature, 2h

With pyridine; potassium hydroxide; In pyridine;

Reference yield:

: 14588-61-5
4-benzyloxy-3,5-dimethoxybenzoic acid chloride

: 92831-90-8
2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1. 1h, 50-60 deg C, 2. 2-3h, room temperature

2: 0.7 g / potassium hydroxide / pyridine / 1. 30 min, 45-50 deg C, 2. room temperature, 2h

With pyridine; potassium hydroxide; In pyridine;

Reference yield:

: 92831-90-8
2-hydroxy-4'-benzyloxy-3,4,5,6,3',5'-hexamethoxydibenzoylmethane

: 85644-03-7
4'-Hydroxy-5,6,7,8,3',5'-hexamethoxyflavone

Guidance literature:: Multi-step reaction with 2 steps

1: 0.4 g / sodium acetate / acetic acid / 3 h / Heating

2: 0.15 g / H₂ / 10percent Pd/C / ethyl acetate

With hydrogen; sodium acetate; palladium on activated charcoal; In acetic acid; ethyl acetate;