Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)-

Base Information

Chemical Name:Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)-
CAS No.:14588-61-5
Molecular Formula:C16H15ClO4
Molecular Weight:306.746
Hs Code.:
DSSTox Substance ID:DTXSID00437650
Wikidata:Q82253189
Mol file:14588-61-5.mol

Synonyms:14588-61-5;Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)-;SCHEMBL10429197;DTXSID00437650;HZFKKOUPDNWXPX-UHFFFAOYSA-N;4-benzyloxy-3,5-dimethoxybenzoic acid chloride

Suppliers and Price of Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)-

Chemical Property:

Vapor Pressure:0mmHg at 25°C
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:306.0658866
Heavy Atom Count:21
Complexity:316

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OCC2=CC=CC=C2)OC)C(=O)Cl

Technology Process of Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)-

There total 8 articles about Benzoyl chloride, 3,5-dimethoxy-4-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 14588-60-4
4-(benzyloxy)-3,5-dimethoxybenzoic acid

: 14588-61-5
4-benzyloxy-3,5-dimethoxybenzoic acid chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 100-39-0
benzyl bromide

: 14588-61-5
4-benzyloxy-3,5-dimethoxybenzoic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: Bu₄NHSO₄, K₂CO₃ / toluene / 6 h / Heating

2: 2M aq. NaOH / various solvent(s) / 0.25 h

3: thionyl chloride / 2 h / Heating

With sodium hydroxide; thionyl chloride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In toluene;
DOI:10.1021/jm00012a012

Reference yield:

: 530-57-4
3,5-dimethoxy-4-hydroxybenzoic acid

: 14588-61-5
4-benzyloxy-3,5-dimethoxybenzoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH-solution

2: benzene; phosphorus pentachloride / 0 °C

With sodium hydroxide; phosphorus pentachloride; benzene;