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Ph3AsAlCl3

Base Information
  • Chemical Name:Ph3AsAlCl3
  • CAS No.:1237071-29-2
  • Molecular Formula:C18H15AlAsCl3
  • Molecular Weight:439.579
  • Hs Code.:
Ph<sub>3</sub>AsAlCl<sub>3</sub>

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Chemical Property of Ph3AsAlCl3
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Technology Process of Ph3AsAlCl3

There total 1 articles about Ph3AsAlCl3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In CH2Cl2; (N2, glovebox); addn. of CH2Cl2 soln. of arsine deriv. to CH2Cl2 soln. of aluminium deriv., stirring for 30 min; layering with hexane, keeping overnight at -25°C, isolation of ppt., washing with ether, recrystn. by layering CH2Cl2 soln. with hexane at -25°C for 48 h, IR and NMR;
DOI:10.1139/V10-029
upstream raw materials:

aluminium trichloride

triphenyl-arsane

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