2-β-benzyloxytilivalline

Base Information

Chemical Name:2-β-benzyloxytilivalline
CAS No.:136024-68-5
Molecular Formula:C₂₇H₂₅N₃O₃
Molecular Weight:439.514
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-β-benzyloxytilivalline

Chemical Property:

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Technology Process of 2-β-benzyloxytilivalline

There total 11 articles about 2-β-benzyloxytilivalline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63478-14-8
2-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)-6-methoxyaniline

: 136024-68-5
2-β-benzyloxytilivalline

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / red phosphorus, 55percent hydriodic acid / 14 h / 100 °C

2: diethyl phosphorocyanidate, N,N-diisopropylethylamine / dimethylformamide / 1) 0 deg C, 1 h, 2) r.t., 2 h

With phosphorus; diethyl cyanophosphonate; hydrogen iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80968-6

Reference yield:

: 100-39-0
benzyl bromide

: 136024-68-5
2-β-benzyloxytilivalline

Guidance literature:: Multi-step reaction with 7 steps

1: 4.52 g / silver oxide / dimethylformamide / 1) 0 deg C, 5 min, 2) r.t., 24 h

2: 56 percent / LiCl, sodium borohydride, EtOH / tetrahydrofuran / 1) 0 deg C, 1 h, 2) r.t., 19.5 h

3: 84 percent / sulfur trioxide-pyridine complex, DMSO, Et₃N / CH₂Cl₂ / 0.17 h / 10 - 20 °C

4: 65 percent / 0.4 M cerium chloride / ethanol / 21 h / 55 °C

5: 10percent HCl / ethanol / 1 h / Ambient temperature

6: diethyl phosphorocyanidate, N,N-diisopropylethylamine / dimethylformamide / 1) 0 deg C, 1 h, 2) r.t., 2 h

With hydrogenchloride; sodium tetrahydroborate; cerium(III) chloride; ethanol; diethyl cyanophosphonate; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; silver(l) oxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80968-6

Reference yield:

: 74844-91-0
1-tert-butyl 2-methyl (2S,4R)-4-hydroxy-1,2-pyrrolidinedicarboxylate

: 136024-68-5
2-β-benzyloxytilivalline

Guidance literature:: Multi-step reaction with 7 steps

1: 4.52 g / silver oxide / dimethylformamide / 1) 0 deg C, 5 min, 2) r.t., 24 h

2: 56 percent / LiCl, sodium borohydride, EtOH / tetrahydrofuran / 1) 0 deg C, 1 h, 2) r.t., 19.5 h

3: 84 percent / sulfur trioxide-pyridine complex, DMSO, Et₃N / CH₂Cl₂ / 0.17 h / 10 - 20 °C

4: 65 percent / 0.4 M cerium chloride / ethanol / 21 h / 55 °C

5: 10percent HCl / ethanol / 1 h / Ambient temperature

6: diethyl phosphorocyanidate, N,N-diisopropylethylamine / dimethylformamide / 1) 0 deg C, 1 h, 2) r.t., 2 h

With hydrogenchloride; sodium tetrahydroborate; cerium(III) chloride; ethanol; diethyl cyanophosphonate; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; silver(l) oxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80968-6