Technology Process of 4-(α(2-methoxyethoxy)3-methoxybenzyl)-2,2-dimethyldioxolane
There total 5 articles about 4-(α(2-methoxyethoxy)3-methoxybenzyl)-2,2-dimethyldioxolane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: vanadyl acetoacetate, t-butyl hydroperoxide / benzene; toluene / 3 h / 60 °C
2: p-toluenesulphonic acid
3: p-toluenesulphonic acid / benzene / Heating
With
tert.-butylhydroperoxide; vanadyl acetoacetonate; toluene-4-sulfonic acid;
In
toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: SOCl2 / CH2Cl2 / Ambient temperature
2: NaBH4, Na2CO3 / acetonitrile; H2O / Ambient temperature
3: vanadyl acetoacetate, t-butyl hydroperoxide / benzene; toluene / 3 h / 60 °C
4: p-toluenesulphonic acid
5: p-toluenesulphonic acid / benzene / Heating
With
tert.-butylhydroperoxide; sodium tetrahydroborate; thionyl chloride; vanadyl acetoacetonate; sodium carbonate; toluene-4-sulfonic acid;
In
dichloromethane; water; toluene; acetonitrile; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaBH4, Na2CO3 / acetonitrile; H2O / Ambient temperature
2: vanadyl acetoacetate, t-butyl hydroperoxide / benzene; toluene / 3 h / 60 °C
3: p-toluenesulphonic acid
4: p-toluenesulphonic acid / benzene / Heating
With
tert.-butylhydroperoxide; sodium tetrahydroborate; vanadyl acetoacetonate; sodium carbonate; toluene-4-sulfonic acid;
In
water; toluene; acetonitrile; benzene;
