(Fe(CH₃C₆H₄SO₃)(C₃₂H₁₆N₈))

Base Information

• Chemical Name: (Fe(CH₃C₆H₄SO₃)(C₃₂H₁₆N₈))
• CAS No.: 23388-23-0
• Molecular Formula: C₃₉H₂₃FeN₈O₃S
• Molecular Weight: 739.576
• Mol file: 23388-23-0.mol

Synonyms:

Chemical Property of (Fe(CH₃C₆H₄SO₃)(C₃₂H₁₆N₈))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Fe(CH₃C₆H₄SO₃)(C₃₂H₁₆N₈))

There total 4 articles about (Fe(CH₃C₆H₄SO₃)(C₃₂H₁₆N₈)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iron(III)phthalocyanine chloride (14285-56-4) + toluene-4-sulfonic acid (104-15-4) → (Fe(CH3C6H4SO3)(C32H16N8)) (23388-23-0,32105-74-1)

Guidance literature:

With KOH; In methanol; acetone; stirring of Fe-compd. and KOH in MeOH/acetone at 40°C for 30 min, filtn., addn. of sulfonic acid; filtn., washing with acetone and water, elem. anal.;

Reference yield:

{N(P(C6H5)3)2}(1+)*{Fe(OH)2(C32H16N8)}(1-)={N(P(C6H5)3)2}{Fe(OH)2(C32H16N8)} + toluene-4-sulfonic acid (104-15-4) → (Fe(CH3C6H4SO3)(C32H16N8)) (23388-23-0,32105-74-1)

Guidance literature:

In dichloromethane; addn. of sulfonic acid to a soln. of Fe-complex under Ar; centrifugation, washing with deoxygenated CH2Cl2, vac. drying;

Reference yield:

Fe(C8H4N2)4CH2CH2N(C6H5)CH3*0.25C4H8O + toluene-4-sulfonic acid (104-15-4) → (Fe(CH3C6H4SO3)(C32H16N8)) (23388-23-0,32105-74-1)

Guidance literature:

In tetrahydrofuran; byproducts: CH2CH2, PhMeNH; (Ar), to Fe-complex dissolved in THF C7H7SO3H in THF added with stirring within 3-10 min; methanolic KOH added, chromd., filtered, washed with water, methanol and ether;

upstream raw materials:

iron(III)phthalocyanine chloride

toluene-4-sulfonic acid