N,N,N-triethylethanaminium tetraphenylborate(1-)

Base Information

• Chemical Name: N,N,N-triethylethanaminium tetraphenylborate(1-)
• CAS No.: 12099-10-4
• Molecular Formula: C24H20B.C8H20N
• Molecular Weight: 449.487
• Mol file: 12099-10-4.mol

Synonyms:

Chemical Property of N,N,N-triethylethanaminium tetraphenylborate(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N,N-triethylethanaminium tetraphenylborate(1-)

There total 3 articles about N,N,N-triethylethanaminium tetraphenylborate(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

tetraethylammonium hexacarbonyltantalate (67292-38-0) + sodium tetraphenyl borate (143-66-8) → Na(1+)*Ta(CO)6(1-) = Na(Ta(CO)6) (15602-40-1) + tetraethylammonium tetraphenylborate (12099-10-4)

Guidance literature:

In methanol; a methanolic slurry of the tantalate treating with a soln. of NaBPh4, stirring for 0.5 h at 40°C and for 1.5 h at 25°C, ammonium borate filtering off, filtrate evapg. to dryness, dissolving in Et2O, filtering, evapg., washing with pentane; identified by elem. anal. and IR spectrum;

Reference yield:

sodium tetraphenyl borate (143-66-8) → tetraethylammonium tetraphenylborate (12099-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) CH₂Cl₂, (ii) /BRN= 3599783/, acetone

2: acetone-d6

In acetone;

DOI:10.1246/bcsj.49.3601

Reference yield:

Aethoxydimorpholinosulfonium-Tetraphenylborat (62432-82-0) + triethylamine (121-44-8) → tetraethylammonium tetraphenylborate (12099-10-4)

Guidance literature:

In acetone;

DOI:10.1246/bcsj.49.3601

upstream raw materials:

Aethoxydimorpholinosulfonium-Tetraphenylborat

triethylamine

sodium tetraphenyl borate

tetraethylammonium hexacarbonyltantalate