tetraethylammonium hexacarbonyltantalate

Base Information

Chemical Name:tetraethylammonium hexacarbonyltantalate
CAS No.:67292-38-0
Molecular Formula:C₆O₆Ta*C₈H₂₀N
Molecular Weight:479.264
Hs Code.:

Synonyms:tetraethylammonium hexacarbonyltantalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylammonium hexacarbonyltantalate

Chemical Property:

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Technology Process of tetraethylammonium hexacarbonyltantalate

There total 1 articles about tetraethylammonium hexacarbonyltantalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 111532-96-8
cis-{(C₂H₅)4N}{Ta(CO)4P{CH₂CH₂P(C₆H₅)2}3}

: 67292-38-0
tetraethylammonium hexacarbonyltantalate

: 111532-97-9
{Ta(H)(CO)3P{CH₂CH₂P(C₆H₅)2}3}

Guidance literature:: In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); soln. of educt, exchange of cation on silica gel (eluent: THF, 20-30min)fraction concd. in vac. at room temp., dropwise addn. of pentane, pptn., filtration, under N2 in O2-free solvent; ppt. washed with pentane, dried in high vac., 4h;
DOI:10.1016/0022-328X(87)80022-0

Reference yield: 90.0%

: 67292-38-0
tetraethylammonium hexacarbonyltantalate

: 2008-61-9
2,6-diisopropylphenylisocyanide

: 7553-56-2,12190-71-5,8031-47-8
iodine

: hexakis(2,6-diisopropylphenyl isocyanide-κC)iodidotantalum(I)

Guidance literature:: tetraethylammonium hexacarbonyltantalate; iodine; In tetrahydrofuran; at -60 - 0 ℃; Inert atmosphere; Molecular sieve;

2,6-diisopropylphenylisocyanide; In tetrahydrofuran; at -60 - 20 ℃; for 2.5h; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.201706323

Reference yield: 86.0%

: 14104-20-2
silver tetrafluoroborate

: 67292-38-0
tetraethylammonium hexacarbonyltantalate

: 2008-61-9
2,6-diisopropylphenylisocyanide

: C₉₁H₁₁₉N₇Ta⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: In tetrahydrofuran; at -60 - 20 ℃; for 12h; Inert atmosphere; Molecular sieve; Schlenk technique;
DOI:10.1002/anie.201706323