diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate

Base Information

Chemical Name:diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate
CAS No.:87363-67-5
Molecular Formula:C₂₃H₃₂N₂O₇
Molecular Weight:448.516
Hs Code.:

Synonyms:

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Chemical Property of diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate

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Technology Process of diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate

There total 3 articles about diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 498-94-2
isonipecotic acid

: 87363-67-5
diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium bicarbonate; 6N HCl / H₂O; diethyl ether / 4 h / Ambient temperature

2: 1) ethyl chloroformate, triethylamine; / 1) ethyl acetate, room temp.,1 h; 2) room temp., 2 h

With hydrogenchloride; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; In diethyl ether; water;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 87363-67-5
diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium bicarbonate; 6N HCl / H₂O; diethyl ether / 4 h / Ambient temperature

2: 1) ethyl chloroformate, triethylamine; / 1) ethyl acetate, room temp.,1 h; 2) room temp., 2 h

With hydrogenchloride; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; In diethyl ether; water;

Reference yield:

: 16450-41-2
L-glutamic acid diethyl ester

: 10314-98-4
1-benzyloxycarbonylpiperidine-4-carboxylic acid

: 87363-67-5
diethyl N-(N-benzyloxycarbonylisonipecotinoyl)-L-glutamate

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1) ethyl acetate, room temp.,1 h; 2) room temp., 2 h;