methyl N-(p-nitrophenyl)-o-nitrobenzimidate

Base Information

• Chemical Name: methyl N-(p-nitrophenyl)-o-nitrobenzimidate
• CAS No.: 109773-12-8
• Molecular Formula: C₁₄H₁₁N₃O₅
• Molecular Weight: 301.258
• Mol file: 109773-12-8.mol

Synonyms:

Chemical Property of methyl N-(p-nitrophenyl)-o-nitrobenzimidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl N-(p-nitrophenyl)-o-nitrobenzimidate

There total 3 articles about methyl N-(p-nitrophenyl)-o-nitrobenzimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

methanol (67-56-1) + N-(2-nitrobenzylidene)-4-nitroaniline (17064-86-7) → methyl N-(p-nitrophenyl)-o-nitrobenzimidate (109773-12-8)

Guidance literature:

With potassium cyanide; for 3h; Heating;

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → methyl N-(p-nitrophenyl)-o-nitrobenzimidate (109773-12-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-p-sulphonic acid / benzene

2: 31 percent / potassium cyanide / 3 h / Heating

With potassium cyanide; toluene-4-sulfonic acid; In benzene;

Reference yield:

2-nitro-benzaldehyde (552-89-6) → methyl N-(p-nitrophenyl)-o-nitrobenzimidate (109773-12-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-p-sulphonic acid / benzene

2: 31 percent / potassium cyanide / 3 h / Heating

With potassium cyanide; toluene-4-sulfonic acid; In benzene;

upstream raw materials:

methanol

N-(2-nitrobenzylidene)-4-nitroaniline

4-nitro-aniline

2-nitro-benzaldehyde