trans-4-MethoxycyclohexanaMine

Base Information

• Chemical Name: trans-4-MethoxycyclohexanaMine
• CAS No.: 121588-79-2
• Molecular Formula: C7H15NO
• Molecular Weight: 129.202
• Hs Code.: 2922199090
• Mol file: 121588-79-2.mol

Synonyms:trans-4-Methoxycyclohexanamine

Chemical Property of trans-4-MethoxycyclohexanaMine

Chemical Property:

• Boiling Point: 174.5±33.0 °C(Predicted)
• PKA: 10.38±0.70(Predicted)
• PSA: 35.25000
• Density: 0.94±0.1 g/cm3(Predicted)
• LogP: 1.60300
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

99%, ^*data from raw suppliers

Trans-4-methoxycyclohexanamine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trans-4-MethoxycyclohexanaMine

There total 5 articles about trans-4-MethoxycyclohexanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-aniline (104-94-9) → methoxycyclohexanamine hydrochloride (121588-79-2) + (cis)-4-methoxycyclohexanamine hydrochloride (130290-78-7)

Guidance literature:

With hydrogen; In 1,4-dioxane; at 100 ℃; for 3.33333h; under 15001.5 Torr; Autoclave;

DOI:10.1016/j.cclet.2020.05.045

Reference yield:

(1r,4r)-N,N-dibenzyl-4-methoxycyclohexan-1-amine → methoxycyclohexanamine hydrochloride (121588-79-2)

Guidance literature:

With 20% palladium hydroxide-activated charcoal; hydrogen; In ethanol; at 20 ℃;

Reference yield:

4-Methoxycyclohexanon-oxim (61367-42-8) → methoxycyclohexanamine hydrochloride (121588-79-2)

Guidance literature:

With sodium ethanolate; In ethanol;

DOI:10.1021/jm00212a019

upstream raw materials:

4-Methoxycyclohexanon-oxim

4-methoxy-phenol

4-methoxy-aniline

trans-4-(dibenzylamino)cyclohexanol

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