Cis-4-methoxycyclohexanamine

Base Information

• Chemical Name: Cis-4-methoxycyclohexanamine
• CAS No.: 130290-78-7
• Molecular Formula: C7H15NO
• Molecular Weight: 129.202
• Hs Code.: 2922199090
• Mol file: 130290-78-7.mol

Synonyms:

Chemical Property of Cis-4-methoxycyclohexanamine

Chemical Property:

• Boiling Point: 174.5±33.0 °C(Predicted)
• PKA: 10.38±0.70(Predicted)
• PSA: 35.25000
• Density: 0.94±0.1 g/cm3(Predicted)
• LogP: 1.60300

Purity/Quality:

98%min ^*data from raw suppliers

Cis-4-methoxycyclohexanamine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cis-4-methoxycyclohexanamine

There total 3 articles about Cis-4-methoxycyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-aniline (104-94-9) → methoxycyclohexanamine hydrochloride (121588-79-2) + (cis)-4-methoxycyclohexanamine hydrochloride (130290-78-7)

Guidance literature:

With hydrogen; In 1,4-dioxane; at 100 ℃; for 3.33333h; under 15001.5 Torr; Autoclave;

DOI:10.1016/j.cclet.2020.05.045

Reference yield:

4-Methoxycyclohexanon-oxim (61367-42-8) → (cis)-4-methoxycyclohexanamine hydrochloride (130290-78-7)

Guidance literature:

With hydrogen; platinum(IV) oxide; In acetic acid;

DOI:10.1021/jm00212a019

Reference yield:

4-methoxy-phenol (150-76-5) → methoxycyclohexanamine hydrochloride (121588-79-2) + (cis)-4-methoxycyclohexanamine hydrochloride (130290-78-7)

Guidance literature:

With alumina-supported nickel; ammonia; hydrogen; In toluene; at 160 ℃; for 3h; Overall yield = 92 percentChromat.; High pressure;

DOI:10.1039/c9gc02625h

upstream raw materials:

4-Methoxycyclohexanon-oxim

4-methoxy-phenol

4-methoxy-aniline

Downstream raw materials:

C₁₀H₁₈ClN₃O₃

1-(2-Chloro-ethyl)-3-(4-methoxy-cyclohexyl)-urea

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