hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V)

Base Information

Chemical Name:hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V)
CAS No.:58441-02-4
Molecular Formula:C₄₄H₂₉N₄O₂W
Molecular Weight:829.59
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V)

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Technology Process of hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V)

There total 4 articles about hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 13283-01-7
tungsten(VI) chloride

: 58441-02-4
hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V)

Guidance literature:: In further solvent(s); meso-tetraphenylporphine was refluxed with WCl6 in phenol at 454 K for 4h; monitored by UV; phenol dist. off by vac.; dissolved in CHCl3; placed onan Al2O3 column; purified twice by chromy.;

Reference yield: 60.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 13283-01-7
tungsten(VI) chloride

: 108-95-2,27073-41-2
phenol

: 58441-02-4
hydroxyoxo(5,10,15,20-tetraphenylporphinato)tungsten(V)

Guidance literature:: In further solvent(s); porphin refluxed with WCl6 in phenol at 454 K for 4 h; according to T. N. Lomova, N. I. Volkova, B. D. Berezin, Zh. Neorg. Khim., 1985, 30 (3), 626; vac. evapd.; dissolved in CHCl3; purified by column chromy. (Al2O3, CHCl3);
DOI:10.1134/S0036023610050116