PhCH₂Co(dmgH)(dpgH)(Py)

Base Information Edit

Chemical Name:PhCH₂Co(dmgH)(dpgH)(Py)
CAS No.:281669-15-6
Molecular Formula:C₃₀H₃₀CoN₅O₄
Molecular Weight:583.593
Hs Code.:
Mol file:281669-15-6.mol

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Chemical Property of PhCH₂Co(dmgH)(dpgH)(Py) Edit

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Technology Process of PhCH₂Co(dmgH)(dpgH)(Py)

There total 8 articles about PhCH₂Co(dmgH)(dpgH)(Py) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: trans-bis(dimethylglyoximato)(pyridine)chlorocobalt(III)

: trans-bis(diphenylglyoximato)(pyridine)chlorocobalt(III)

: 100-44-7
benzyl chloride

: trans-bis(dimethylglyoximato)(pyridine)benzylcobalt(III)

: 281669-15-6
(benzyl)Co(dimethylglyoximato)(diphenylglyoximato)(pyridine)

: 63463-70-7
trans-bis(diphenylglyoximato)(pyridine)benzylcobalt(III)

Guidance literature:: With NaOH; NaBH₄; In methanol; water; addn. of aq. soln. of NaOH to a suspn. of cobalt complexes in CH3OH, purging with argon for 15 min, cooling to 0°C, addn. of a soln. of NaBH4 in CH3OH, stirring for 30 min, addn. of a soln. of ligand in CH3OH,stirring for 15 min in the dark; pouring into water, filtration, drying, column chromy (SiO2, ethylacetate/CHCl3);
DOI:10.1016/S0022-328X(01)00731-8