C₁₃H₁₈OS₂

Base Information

• Chemical Name: C₁₃H₁₈OS₂
• CAS No.: 1450842-94-0
• Molecular Formula: C₁₃H₁₈OS₂
• Molecular Weight: 254.417
• Mol file: 1450842-94-0.mol

Synonyms:

Chemical Property of C₁₃H₁₈OS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₃H₁₈OS₂

There total 2 articles about C₁₃H₁₈OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H16OS2 + methyl iodide (74-88-4) → C13H18OS2 (1450842-94-0)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1039/c3ob40685g

Reference yield:

phenylacetaldehyde (122-78-1) → C13H18OS2 (1450842-94-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -20 °C

1.2: 0 °C

2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;

DOI:10.1039/c3ob40685g

Reference yield:

C13H18OS2 (1450842-94-0) → 2-methoxy-3-phenylpropanal (256229-07-9)

Guidance literature:

With N-Bromosuccinimide; barium carbonate; In acetone; at 0 - 30 ℃;

DOI:10.1039/c3ob40685g

upstream raw materials:

phenylacetaldehyde

methyl iodide

Downstream raw materials:

2-methoxy-3-phenylpropanal