N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride

Base Information

• Chemical Name: N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride
• CAS No.: 1253390-70-3
• Molecular Formula: C₃₀H₃₃N₆O₄*Cl
• Molecular Weight: 577.083
• Mol file: 1253390-70-3.mol

Synonyms:

Chemical Property of N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride

There total 1 articles about N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dmap (1122-58-3) + tert-butyl allyl-(4-(benzyloxy)-7-chloro-6-formylpyrido[2,3-d]pyrimidin-2-yl)carbamate (1253390-67-8) → N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride (1253390-70-3)

Guidance literature:

In acetonitrile; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo101194v

Reference yield: 20.0%

N-(1-(2-(allyl(tert-butoxycarbonyl)amino)-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-7-yl)pyridin-4(1H)-ylidene)-N-methylmethanaminium chloride (1253390-70-3) → tert-butyl allyl-(7-amino-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-2-yl)carbamate (1253390-69-0)

Guidance literature:

In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo101194v

upstream raw materials:

dmap

tert-butyl allyl-(4-(benzyloxy)-7-chloro-6-formylpyrido[2,3-d]pyrimidin-2-yl)carbamate

Downstream raw materials:

tert-butyl allyl-(7-amino-4-(benzyloxy)-6-formylpyrido[2,3-d]pyrimidin-2-yl)carbamate