heptacyclo[6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14]tetradecanone

Base Information

• Chemical Name: heptacyclo[6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14]tetradecanone
• CAS No.: 119347-55-6
• Molecular Formula: C₁₄H₁₄O
• Molecular Weight: 198.265

Synonyms:

Chemical Property of heptacyclo[6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14]tetradecanone

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Technology Process of heptacyclo[6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14]tetradecanone

There total 2 articles about heptacyclo[6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14]tetradecanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

heptacyclo<6.6.0.02,6.03,13.04,11.05,9.010,14>tetradecane (17872-39-8) → heptacyclo[6.6.0.02,6.03,13.04,11.05,9.010,14]tetradecanone (119347-55-6) + hexacyclo[6.6.0.02,6.03,13.04,11.05,9]tetradecane-10,14-dione (112533-27-4) + 1-(2'-pyridyl)heptacyclo[6.6.0.02,6.03,13.04,11.05,9.010,14]tetradecane + 1-(4'-pyridyl)heptacyclo[6.6.0.02,6.03,13.04,11.05,9.010,14]te

Guidance literature:

With pyridine; 2-Picolinic acid; tert.-butylhydroperoxide; hexaaquairon(II) perchlorate; oxygen; lithium chloride; ascorbic acid; In water; for 120h; Further byproducts given; Ambient temperature; further oxidizing agents;

DOI:10.1016/S0040-4020(96)01110-6

Reference yield: 7.0%

pyridine (110-86-1) + heptacyclo<6.6.0.02,6.03,13.04,11.05,9.010,14>tetradecane (17872-39-8) → heptacyclo[6.6.0.02,6.03,13.04,11.05,9.010,14]tetradecanone (119347-55-6) + hexacyclo[6.6.0.02,6.03,13.04,11.05,9]tetradecane-10,14-dione (112533-27-4) + 1-(2'-pyridyl)heptacyclo[6.6.0.02,6.03,13.04,11.05,9.010,14]tetradecane + 1-(4'-pyridyl)heptacyclo[6.6.0.02,6.03,13.04,11.05,9.010,14]te

Guidance literature:

With 2-Picolinic acid; tert.-butylhydroperoxide; hexaaquairon(II) perchlorate; oxygen; acetic acid; lithium chloride; In water; for 120h; Further byproducts given; Ambient temperature; further oxidizing agents;

DOI:10.1016/S0040-4020(96)01110-6

upstream raw materials:

pyridine

heptacyclo<6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14>tetradecane

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