Technology Process of C21H24N2O3
There total 4 articles about C21H24N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: C15H24ClNO2Si / dichloromethane / 0.17 h / Inert atmosphere
1.2: 1.5 h / 0 °C / Inert atmosphere
2.1: basic alumina / ethyl acetate / Inert atmosphere
With
C15H24ClNO2Si;
In
dichloromethane; ethyl acetate;
1.1: Mannich reaction / 1.2: Mannich reaction;
DOI:10.1021/ol103096u
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: titanium(IV) isopropylate / tetrahydrofuran / 14 h / Inert atmosphere
2.1: C15H24ClNO2Si / dichloromethane / 0.17 h / Inert atmosphere
2.2: 1.5 h / 0 °C / Inert atmosphere
3.1: basic alumina / ethyl acetate / Inert atmosphere
With
titanium(IV) isopropylate; C15H24ClNO2Si;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
2.1: Mannich reaction / 2.2: Mannich reaction;
DOI:10.1021/ol103096u
- Guidance literature:
-
With
basic alumina;
In
ethyl acetate;
Inert atmosphere;
DOI:10.1021/ol103096u