HC[SiMe₂N(4-MeC₆H₄)]3B

Base Information

Chemical Name:HC[SiMe₂N(4-MeC₆H₄)]3B
CAS No.:929197-44-4
Molecular Formula:C₂₈H₄₀BN₃Si₃
Molecular Weight:513.713
Hs Code.:

HC[SiMe<sub>2</sub>N(4-MeC<sub>6</sub>H<sub>4</sub>)]3B

Synonyms:

Suppliers and Price of HC[SiMe₂N(4-MeC₆H₄)]3B

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of HC[SiMe₂N(4-MeC₆H₄)]3B

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of HC[SiMe₂N(4-MeC₆H₄)]3B

There total 1 articles about HC[SiMe₂N(4-MeC₆H₄)]3B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 156053-42-8
CH[(CH₃)2SiNH(p-tolyl)]3

: 10294-34-5
boron trichloride

: 929197-44-4
HC[SiMe₂N(4-MeC₆H₄)]3B

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; byproducts: HC(Si(CH3)2N(C6H4CH3))3Li3*2(C2H5)2O; n-C4H9Li in hexanes added to a soln. of HC(Si(CH3)2NH(C6H4CH3))3 in hexanes/ether at -50°C, warmed slowly to room temp. and stirred for 5h, cooled to -78°C, BCl3 in hexanes added, warmed gradually to a mbient temp. while stirring overnight; filtered, concd., crystd. at -30°C for 3 d, sepd., dried (vac.); elem. anal.;
DOI:10.1021/ic0620889

Reference yield: 95.0%

: rac-ethylenebis(1-indenyl)zirconium dimethyl

: 929197-44-4
HC[SiMe₂N(4-MeC₆H₄)]3B

: 958228-61-0
((C₉H₆)2C₂H₄)Zr(CH₃)NC₆H₄CH₃Si(CH₃)2HC(Si(CH₃)2NC₆H₄CH₃)2BCH₃

Guidance literature:: In toluene; (Ar) the mixt. of Zr-complex and B-compound in toluene was stirred for 10 min at ambient temp.; evapd. to dryness under vac., the residue was extd. with hexanes and filtered, evapd. to dryness; elem. anal.;
DOI:10.1021/om700587w

Reference yield: 95.0%

: 12636-72-5
bis(cyclopentadienyl)dimethylzirconium(IV)

: 929197-44-4
HC[SiMe₂N(4-MeC₆H₄)]3B

: (C₅H₅)2Zr(CH₃)NC₆H₄CH₃Si(CH₃)2HC(Si(CH₃)2NC₆H₄CH₃)2BCH₃

Guidance literature:: In toluene; (Ar) the mixt. of Zr-complex and B-compound in toluene was stirred for 10 min at ambient temp.; evapd. to dryness under vac., the residue was extd. with hexanes and filtered, evapd. to dryness; elem. anal.;
DOI:10.1021/om700587w