cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

Base Information

Chemical Name:cis-3-Methyl-5-phenyl-1-methylidenecyclohexane
CAS No.:60741-75-5
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:

Suppliers and Price of cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

There total 14 articles about cis-3-Methyl-5-phenyl-1-methylidenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7214-50-8
5-methylcyclohex-2-en-1-one

: 28557-00-8
phenylzinc chloride

: 28467-39-2,28467-40-5,60741-75-5
cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

: 28467-40-5
trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 0 ℃; for 0.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol300387f

Reference yield:

: 7214-50-8
5-methylcyclohex-2-en-1-one

: 98-80-6
phenylboronic acid

: 28467-39-2,28467-40-5,60741-75-5
cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

: 28467-40-5
trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Guidance literature:: With [Rh(OH)(cod)]2; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; water; at 35 ℃; for 4h; optical yield given as %de;
DOI:10.1021/ol300387f

Reference yield:

: C₂₀H₂₃BrS

: 28467-39-2,28467-40-5,60741-75-5
cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

: 28467-40-5
trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Guidance literature:: With benzophenone; hexamethyldistannane; In benzene-d6; at 40 ℃; for 20h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;
DOI:10.1021/jo00129a024