(Ph₃P)₃AgOAc

Base Information

Chemical Name:(Ph₃P)₃AgOAc
CAS No.:66083-58-7
Molecular Formula:C₅₆H₄₈AgO₂P₃
Molecular Weight:953.785
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Ph₃P)₃AgOAc

Chemical Property:

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Technology Process of (Ph₃P)₃AgOAc

There total 2 articles about (Ph₃P)₃AgOAc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 563-63-3
silver(I) acetate

: 603-35-0
triphenylphosphine

: 66083-58-7
O,O'-acetatotris(triphenylphosphine)silver(I)

Guidance literature:: In toluene; AgCH3CO2 was added to PPh3 in toluene, stirred in the dark for 24 h; filtered in air, dried in vacuo; elem. anal.;
DOI:10.1016/S0020-1693(01)00718-6

Reference yield:

: 563-63-3
silver(I) acetate

: 66083-58-7
(Ph₃P)₃AgOAc

Guidance literature:: With triphenylphosphine; In benzene; dissoln. of Ag-salt into slight stoich. excess of PPh3-soln.; pptn. on pentane addn., filtration, washing (pentane), drying (vac.); elem. anal.;
DOI:10.1039/DT9770002068

Reference yield:

: 66083-58-7
(Ph₃P)₃AgOAc

: 66083-49-6,74344-98-2
O,O'-acetatobis(triphenylphosphine)silver(I)

Guidance literature:: In chloroform; byproducts: PPh3; refluxing; solvent removal, filtration, washing (Et2O), drying (vac.); elem. anal.;
DOI:10.1039/DT9770002068