3-Bromo-2,4-dimethoxybenzaldehyde

Base Information

Chemical Name:3-Bromo-2,4-dimethoxybenzaldehyde
CAS No.:122452-59-9
Molecular Formula:C9H9BrO3
Molecular Weight:245.073
Hs Code.:
DSSTox Substance ID:DTXSID60556210
Wikidata:Q82437704

Synonyms:3-bromo-2,4-dimethoxybenzaldehyde;122452-59-9;Benzaldehyde, 3-bromo-2,4-dimethoxy-;SCHEMBL1534505;DTXSID60556210;QXSWWYIZFZHXNS-UHFFFAOYSA-N;3-bromo-2,4-dimethoxy-benzaldehyde;EN300-5258126;Z1416160493

Suppliers and Price of 3-Bromo-2,4-dimethoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Bromo-2,4-dimethoxybenzaldehyde

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:243.97351
Heavy Atom Count:13
Complexity:174

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)C=O)OC)Br

Technology Process of 3-Bromo-2,4-dimethoxybenzaldehyde

There total 4 articles about 3-Bromo-2,4-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 63638-85-7
3-bromo-2-hydroxy-4-methoxybenzaldehyde

: 74-88-4
methyl iodide

: 122452-59-9
3-bromo-2,4-dimethoxybenzaldehyde

Guidance literature:: With potassium carbonate;
DOI:10.1016/S0040-4039(00)80501-8

Reference yield:

: 4885-02-3
Dichloromethyl methyl ether

: 16932-45-9
1-bromo-2,6-dimethoxybenzene

: 122452-59-9
3-bromo-2,4-dimethoxybenzaldehyde

Guidance literature:: With titanium tetrachloride; Yield given. Multistep reaction; 1.) CH₂Cl₂, -40 deg C, 2.) 0 deg C;
DOI:10.1002/hlca.19900730105

Reference yield:

: 673-22-3
2-Hydroxy-4-methoxybenzaldehyde

: 122452-59-9
3-bromo-2,4-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaBr, Hg(OAc)2; 2.) Br₂ / 1.) alcohol,1percent acetic acid, reflux; 2.) CHCl₃, acetic acid

2: 90 percent / K₂CO₃

With mercury(II) diacetate; bromine; potassium carbonate; sodium bromide;
DOI:10.1016/S0040-4039(00)80501-8