9-Ethyl-3-carbazolecarboxaldehyde oxime

Base Information

Chemical Name:9-Ethyl-3-carbazolecarboxaldehyde oxime
CAS No.:122497-48-7
Molecular Formula:C15H14N2O
Molecular Weight:238.28400
Hs Code.:
DSSTox Substance ID:DTXSID60354874
Wikidata:Q27188057
Mol file:122497-48-7.mol

Synonyms:9-ethyl-3-carbazolecarboxaldehyde oxime;122497-48-7;N-[(9-ethylcarbazol-3-yl)methylidene]hydroxylamine;9H-Carbazole-3-carboxaldehyde, 9-ethyl-, oxime;Oprea1_680754;CBDivE_012953;DTXSID60354874;CHEBI:109047;AKOS017263439;Q27188057

Suppliers and Price of 9-Ethyl-3-carbazolecarboxaldehyde oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 9-Ethyl-3-carbazolecarboxaldehyde oxime

Chemical Property:

PSA：37.52000
LogP:3.62250
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:238.110613074
Heavy Atom Count:18
Complexity:318

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN1C2=C(C=C(C=C2)C=NO)C3=CC=CC=C31

Technology Process of 9-Ethyl-3-carbazolecarboxaldehyde oxime

There total 3 articles about 9-Ethyl-3-carbazolecarboxaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7570-45-8
N-ethyl-3-carbazolealdehyde

: 122497-48-7
N-ethylcarbazole-3-carboxaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 20 ℃; for 18h; Reagent/catalyst; Solvent;
DOI:10.1071/CH16169

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 122497-48-7
N-ethylcarbazole-3-carboxaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 18 h / 20 °C

2: titanium tetrachloride / dichloromethane / 4 h / -78 °C

3: hydroxylamine hydrochloride; sodium hydroxide / water; ethanol / 18 h / 20 °C

With hydroxylamine hydrochloride; titanium tetrachloride; sodium hydride; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; 2: |Rieche Formylation;
DOI:10.1071/CH16169

Reference yield:

: 86-28-2
N-ethylcarbazole

: 122497-48-7
N-ethylcarbazole-3-carboxaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetrachloride / dichloromethane / 4 h / -78 °C

2: hydroxylamine hydrochloride; sodium hydroxide / water; ethanol / 18 h / 20 °C

With hydroxylamine hydrochloride; titanium tetrachloride; sodium hydroxide; In ethanol; dichloromethane; water; 1: |Rieche Formylation;
DOI:10.1071/CH16169