((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)

Base Information

Chemical Name:((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)
CAS No.:1202260-13-6
Molecular Formula:C₃₀H₄₅CoO₂P₄
Molecular Weight:620.574
Hs Code.:

Synonyms:

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Chemical Property of ((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)

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Technology Process of ((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)

There total 1 articles about ((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 50777-73-6
2-(ortho-diphenylphosphinophenyl)-1,3-dioxolane

: methyltetrakis(trimethylphosphine)cobalt(I)

: 1202260-13-6
((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)

Guidance literature:: In diethyl ether; byproducts: CH4, P(CH3)3; 2-(2-(diphenylphosphanyl)phenyl)-1,3-dioxalane and Co(CH3)(PMe3)4 combined in Et2O at -70°C; kept at 20°C for 16 h; evapn. in vac.; residue extd. with pentane; crystn. at -27°C; elem. anal.;
DOI:10.1002/zaac.200800309

Reference yield: 74.0%

: 1202260-13-6
((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)

: 201230-82-2
carbon monoxide

: 1202260-15-8
((2-diphenylphosphanyl)-3-benzoyl-(1,3-dioxalane-2-yl)-C,P)(carboynl)bis(trimethyphosphane)cobalt

Guidance literature:: In pentane; byproducts: P(CH3)3; ((CH3)3P)3CoP(C6H5)2C6H3C3H5O2 kept stirring in pentane under 1 bar CO for 16 h; evapn. in vac.; residue extd. with Et2O; crystn. at 4°C; elem. anal.;
DOI:10.1002/zaac.200800309

Reference yield: 38.0%

: 1202260-13-6
((2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)tris(trimethylphosphane)cobalt(I)

: 74-88-4
methyl iodide

: 1202260-14-7
(iodo-methyl-(2-diphenylphosphanyl)-3-phenyl-(1,3-dioxalane-2-yl)-C,P)bis(trimethylphosphane)cobalt

Guidance literature:: In tetrahydrofuran; byproducts: tetramethylphosphonium iodide; ((CH3)3P)3CoP(C6H5)2C6H3C3H5O2 and MeI combined in THF at -70°C; kept 15 h at 20°C; evapn. in vac.; residue extd. with Et2O/pentane; crystn. at 4°C; elem. anal.;
DOI:10.1002/zaac.200800309