dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)

Base Information

• Chemical Name: dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)
• CAS No.: 110181-62-9
• Molecular Formula: C₁₀H₁₂BrCl₂OPS
• Molecular Weight: 362.054

Synonyms:

Chemical Property of dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)

Chemical Property:

Purity/Quality:

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Technology Process of dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)

There total 2 articles about dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-bromo-4-tert-butyl-phenoxy)-dichloro-phosphine (110181-61-8) → dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester) (110181-62-9)

Guidance literature:

With trichlorophosphate;

DOI:10.1021/jo01105a025

Reference yield:

2-bromo-4-tert-butylphenol (2198-66-5) → dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester) (110181-62-9)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₃ / anschliessendes Erwaermen mit MgCl₂

2: PSCl₃

With trichlorophosphate; phosphorus trichloride;

DOI:10.1021/jo01105a025

Reference yield:

dichlorothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester) (110181-62-9) + sodium methylate (124-41-4) → amidothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)-O'-methyl ester (99862-33-6)

Guidance literature:

With benzene; Behandeln des Reaktionsprodukts mit wss. NH₃ und Aceton;

upstream raw materials:

(2-bromo-4-tert-butyl-phenoxy)-dichloro-phosphine

2-bromo-4-tert-butylphenol

Downstream raw materials:

hydrazidothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)-O'-methyl ester

amidothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)-O'-methyl ester

ethyl-amidothiophosphoric acid O-(2-bromo-4-tert-butyl-phenyl ester)-O'-methyl ester

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