C₂₆H₃₂N₆O₂

Base Information

Chemical Name:C₂₆H₃₂N₆O₂
CAS No.:1458639-32-1
Molecular Formula:C₂₆H₃₂N₆O₂
Molecular Weight:460.579
Hs Code.:

C<sub>26</sub>H<sub>32</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₂N₆O₂

Chemical Property:

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Technology Process of C₂₆H₃₂N₆O₂

There total 7 articles about C₂₆H₃₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4421-09-4
piperonylonitrile

: 1458639-32-1
C₂₆H₃₂N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: nitric acid; acetic anhydride / 20 °C

2.1: sodium dithionite; tetrabutylammomium bromide / water; dichloromethane / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl acetamide

3.2: Reflux

4.1: trichlorophosphate; N,N-diethylaniline / acetonitrile / Reflux

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

6.1: neat (no solvent) / 0.5 h / 185 °C / Microwave irradiation

With sodium dithionite; tetrabutylammomium bromide; nitric acid; acetic anhydride; N-ethyl-N,N-diisopropylamine; N,N-diethylaniline; trichlorophosphate; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; acetonitrile;
DOI:10.1039/c4md00274a

Reference yield:

: 52805-38-6
6-nitro-1,3-benzodioxole-5-carbonitrile

: 1458639-32-1
C₂₆H₃₂N₆O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium dithionite; tetrabutylammomium bromide / water; dichloromethane / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl acetamide

2.2: Reflux

3.1: trichlorophosphate; N,N-diethylaniline / acetonitrile / Reflux

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5.1: neat (no solvent) / 0.5 h / 185 °C / Microwave irradiation

With sodium dithionite; tetrabutylammomium bromide; N-ethyl-N,N-diisopropylamine; N,N-diethylaniline; trichlorophosphate; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; acetonitrile;
DOI:10.1039/c4md00274a

Reference yield:

: 1,3-dioxolo<4,5-g>quinazolin-6,8(5H,7H)-dione

: 1458639-32-1
C₂₆H₃₂N₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate; N,N-diethylaniline / acetonitrile / Reflux

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

3: neat (no solvent) / 0.5 h / 185 °C / Microwave irradiation

With N-ethyl-N,N-diisopropylamine; N,N-diethylaniline; trichlorophosphate; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c4md00274a