1,2,3,4-Tetrafluoro-5,6-dinitrobenzene

Base Information

Chemical Name:1,2,3,4-Tetrafluoro-5,6-dinitrobenzene
CAS No.:16582-87-9
Molecular Formula:C₆F₄N₂O₄
Molecular Weight:240.071
Hs Code.:
DSSTox Substance ID:DTXSID401034216
Nikkaji Number:J850.848H

Synonyms:1,2,3,4-tetrafluoro-5,6-dinitrobenzene;1,2-Dinitrotetrafluorobenzene;SCHEMBL18274954;DTXSID401034216;16582-87-9

Suppliers and Price of 1,2,3,4-Tetrafluoro-5,6-dinitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1,2,3,4-Tetrafluoro-5,6-dinitrobenzene

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:0
Exact Mass:239.97941913
Heavy Atom Count:16
Complexity:276

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1(=C(C(=C(C(=C1F)F)F)F)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1,2,3,4-Tetrafluoro-5,6-dinitrobenzene

There total 6 articles about 1,2,3,4-Tetrafluoro-5,6-dinitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6157-98-8
2,3,4,5-tetrafluoro-6-nitroaniline

: 16582-87-9
1,2,3,4-tetrafluoro-5,6-dinitrobenzene

Guidance literature:: With dihydrogen peroxide; trifluoroacetic anhydride; In dichloromethane; Heating;
DOI:10.1016/S0040-4020(01)92570-0

Reference yield:

: 6157-98-8
2,3,4,5-tetrafluoro-6-nitroaniline

: 407-25-0
trifluoroacetic anhydride

: 16582-87-9
1,2,3,4-tetrafluoro-5,6-dinitrobenzene

Guidance literature:: With dihydrogen peroxide; In dichloromethane; with 85% H2O2; heating in reflux 4 h with stirring;
DOI:10.1016/S0040-4020(01)92570-0

Reference yield:

: 880-78-4
pentafluoronitrobenzen

: 16582-87-9
1,2,3,4-tetrafluoro-5,6-dinitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NH₃ / diethyl ether / 18 h / Ambient temperature

2: 85percent aq. H₂O₂, TFA / CH₂Cl₂ / 16 h / Ambient temperature

With ammonia; dihydrogen peroxide; trifluoroacetic acid; In diethyl ether; dichloromethane;
DOI:10.1016/S0022-1139(96)03517-8