2-Methoxy-3.5-dimethyl-benzoylchlorid

Base Information

Chemical Name:2-Methoxy-3.5-dimethyl-benzoylchlorid
CAS No.:21553-48-0
Molecular Formula:C₁₀H₁₁ClO₂
Molecular Weight:198.649
Hs Code.:

Synonyms:

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Chemical Property of 2-Methoxy-3.5-dimethyl-benzoylchlorid

Chemical Property:

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Technology Process of 2-Methoxy-3.5-dimethyl-benzoylchlorid

There total 5 articles about 2-Methoxy-3.5-dimethyl-benzoylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6738-23-4
2,4-dimethylanisole

: 21553-48-0
2-Methoxy-3.5-dimethyl-benzoylchlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 25.6 percent / Br₂; acetic acid / Fe / 5 h / 50 °C

2: 36.8 percent / n-butyl lithium / diethyl ether

3: SOCl₂ / 12 h / Heating

With n-butyllithium; thionyl chloride; bromine; acetic acid; iron; In diethyl ether; 1: Bromination / 2: Carboxylation / 3: Chlorination;
DOI:10.1002/ps.2780410210

Reference yield:

: 105-67-9
2,4-Xylenol

: 21553-48-0
2-Methoxy-3.5-dimethyl-benzoylchlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / NaH / dimethylformamide / 5 h / 20 °C

2: 25.6 percent / Br₂; acetic acid / Fe / 5 h / 50 °C

3: 36.8 percent / n-butyl lithium / diethyl ether

4: SOCl₂ / 12 h / Heating

With n-butyllithium; thionyl chloride; bromine; sodium hydride; acetic acid; iron; In diethyl ether; N,N-dimethyl-formamide; 1: Methylation / 2: Bromination / 3: Carboxylation / 4: Chlorination;
DOI:10.1002/ps.2780410210

Reference yield:

: 65492-45-7
1-bromo-2-methoxy-3,5-dimethylbenzene

: 21553-48-0
2-Methoxy-3.5-dimethyl-benzoylchlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 36.8 percent / n-butyl lithium / diethyl ether

2: SOCl₂ / 12 h / Heating

With n-butyllithium; thionyl chloride; In diethyl ether; 1: Carboxylation / 2: Chlorination;
DOI:10.1002/ps.2780410210