PdCl((C₆H₅)3P)2C₉H₅NCH₃O

Base Information

Chemical Name:PdCl((C₆H₅)3P)2C₉H₅NCH₃O
CAS No.:692775-64-7
Molecular Formula:C₄₆H₃₈ClNOP₂Pd
Molecular Weight:824.634
Hs Code.:

PdCl((C<sub>6</sub>H<sub>5</sub>)3P)2C<sub>9</sub>H<sub>5</sub>NCH<sub>3</sub>O

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Chemical Property of PdCl((C₆H₅)3P)2C₉H₅NCH₃O

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Technology Process of PdCl((C₆H₅)3P)2C₉H₅NCH₃O

There total 1 articles about PdCl((C₆H₅)3P)2C₉H₅NCH₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 32262-17-2
4-chloro-1-methyl-1H-quinolin-2-one

: 692775-64-7
PdCl((C₆H₅)3P)2C₉H₅NCH₃O

Guidance literature:: In benzene; under N2 or Ar; a mixt. of Pd-contg. compd. (1 mmol) and halide (1 mmol)were suspended in benzene and refluxed at 60°C for 3 h; cooling to room temp.; the mixt. was filtered through Celite; pptn. by addn. of hexane; recrystn. from CH2Cl2-hexane (-30°C) followed by filtration and drying in vac.; elem. anal.;

Reference yield: 43.0%

: 692775-64-7
PdCl((C₆H₅)3P)2C₉H₅NCH₃O

: 333-27-7
methyl trifluoromethanesulfonate

: chloro(2-methoxy-N-methylquinolin-4-yl)bis(triphenylphosphine)palladium(II) trifluoromethanesulfonate

Guidance literature:: In tetrahydrofuran; under N2 or Ar; Pd-contg. complex (0.5 mmol) was dissolved in THF and cooled to -60°C; CF3SO3CH3 (0.6 mmol) in THF was added dropwise over 10 min; stirring at -60°C for 1 h; stirring at room temp. for 1h; the THF was evapd. in vac.; the residue was repeatedly washed with diethyl ether; drying overnight under igh vac. (1 mm Hg); elem. anal.;