ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride

Base Information

Chemical Name:ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride
CAS No.:100370-88-5
Molecular Formula:C₁₂H₁₇NO₃S*ClH
Molecular Weight:291.799
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride

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Technology Process of ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride

There total 1 articles about ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 64-17-5
ethanol

: 17087-39-7,17087-40-0,23150-29-0,23150-30-3,50731-18-5
DL-threo-3-(4-methylthiophenyl)serine

: 100370-88-5,139235-94-2,139404-47-0
ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride

Guidance literature:: With hydrogenchloride; at 50 ℃; for 5h;
DOI:10.1055/s-1991-26603

Reference yield:

: 100370-88-5,139235-94-2,139404-47-0
ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride

: 23150-35-8
(R*,R*)-(+)-thiomicamine

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / 35 °C / enzymatic hydrolysis: Streptococcus griseus (immobilized on sepharose, pH 7.5)

2: SOCl₂ / 24 h / -5 - 0 °C

3: 75 percent / CaCl₂, NaBH₄ / ethanol / 2 h / 20 - 25 °C

With sodium tetrahydroborate; thionyl chloride; calcium chloride; In ethanol; water;
DOI:10.1055/s-1991-26603

Reference yield:

: 100370-88-5,139235-94-2,139404-47-0
ethyl DL-threo-3-(4-methylthiophenyl)serinate hydrochloride

: 139164-31-1
methyl D-threo-3-(4-methylthiophenyl)serinate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / 35 °C / enzymatic hydrolysis: Streptococcus griseus (immobilized on sepharose, pH 7.5)

2: SOCl₂ / 24 h / -5 - 0 °C

With thionyl chloride; In water;
DOI:10.1055/s-1991-26603