{(CO)3MoMes}2GaMes

Base Information

Chemical Name:{(CO)3MoMes}2GaMes
CAS No.:120085-50-9
Molecular Formula:C₃₃H₃₃GaMo₂O₆
Molecular Weight:787.224
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {(CO)3MoMes}2GaMes

Chemical Property:

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Technology Process of {(CO)3MoMes}2GaMes

There total 1 articles about {(CO)3MoMes}2GaMes which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 60607-12-7
trimesitylgallium

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 120085-51-0
{(CO)3MoMes}GaMes₂

: 120085-50-9
{(CO)3MoMes}2GaMes

Guidance literature:: In 1,2-dimethoxyethane; byproducts: CO; in vac. or under Ar; refluxing of the mixt. in DME, 24-28h; washed several times (pentane); recrystn. (DME); filtered; washed (DME); evapn.; elem. anal.;

Reference yield:

: 120085-50-9
{(CO)3MoMes}2GaMes

: 12089-15-5
tricarbonylmesitylenemolybdenum⁽⁰⁾

: 120085-58-7
{(CO)3MoMes}2GaCl*THF-d8

: 120085-57-6
{(CO)3MoMes}GaMesCl

Guidance literature:: With HCl; In tetrahydrofuran-d8; byproducts: C6H3(CH3)3; under vac. or Ar ; addn. of THF-d8 by vac. distn.; HCl condensed in at -196°C; mixt. warmed to room temp.; stirred 10 min; not isolated; identified by 1H-NMR;

Reference yield:

: 109391-14-2
mesitylgallium dichloride

: 120085-50-9
{(CO)3MoMes}2GaMes

: 120085-51-0
{(CO)3MoMes}GaMes₂

: 120085-53-2
{(CO)3MoMes}2GaCl*0.5DME

: 120085-54-3
{(CO)3MoMes}GaCl₂*0.5DME

Guidance literature:: In 1,2-dimethoxyethane; byproducts: (C6H2(CH3)3)2GaCl*CH3OCH3; under Ar or vac.; addn. of DME by vac. distn. to MesGaCl2; addn to DME soln. of ((CO)3MoMes)2GaMes at room temp., stirred 4 days at room temp.; filtered; evapn.; redissolved in DME; layered with pentane; left standing 16h yielded crystals; decanted; evapn.; identified by 1H NMR (crystals: ((CO)3MoMes)GaCl2*0.5DME, viscous material((CO)3MoMes)GaMes2, ((CO)3MoMes)2GaCl*DME and Mes2GaCl*DME;