Technology Process of C51H50N2O15
There total 10 articles about C51H50N2O15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
zinc;
In
N,N-dimethyl-formamide;
at 40 - 50 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 27 percent / silver triflate, tetramethyl urea / CH2Cl2 / 1) 3-4 h, -30 deg C, 2) 2-3 d, room temperature
2: 90 percent / NaI / acetone / 15 h / Ambient temperature
3: Zn / dimethylformamide / 40 - 50 °C
With
silver trifluoromethanesulfonate; tetramethylurea; sodium iodide; zinc;
In
dichloromethane; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / thionylchloride / 40 - 50 °C
2: 88 percent / dicyclohexylcarbodiimide, N-hydroxysuccinimide, triethylamine
3: 27 percent / silver triflate, tetramethyl urea / CH2Cl2 / 1) 3-4 h, -30 deg C, 2) 2-3 d, room temperature
4: 90 percent / NaI / acetone / 15 h / Ambient temperature
5: Zn / dimethylformamide / 40 - 50 °C
With
1-hydroxy-pyrrolidine-2,5-dione; thionyl chloride; silver trifluoromethanesulfonate; triethylamine; dicyclohexyl-carbodiimide; tetramethylurea; sodium iodide; zinc;
In
dichloromethane; N,N-dimethyl-formamide; acetone;