rac-2,2,5-trimethyl-5-phenyltetrahydropyran

Base Information

Chemical Name:rac-2,2,5-trimethyl-5-phenyltetrahydropyran
CAS No.:1512853-94-9
Molecular Formula:C₁₄H₂₀O
Molecular Weight:204.312
Hs Code.:

Synonyms:

Suppliers and Price of rac-2,2,5-trimethyl-5-phenyltetrahydropyran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of rac-2,2,5-trimethyl-5-phenyltetrahydropyran

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of rac-2,2,5-trimethyl-5-phenyltetrahydropyran

There total 4 articles about rac-2,2,5-trimethyl-5-phenyltetrahydropyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 97006-05-8
rac-2,5-dimethyl-2-phenylhex-4-en-1-ol

: 1512853-94-9
rac-2,2,5-trimethyl-5-phenyltetrahydropyran

Guidance literature:: With aluminium(III) triflate; In dichloromethane; for 10h; Reflux;
DOI:10.1021/om401070c

Reference yield:

: 34713-70-7
2-Phenylpropanal

: 1512853-94-9
rac-2,2,5-trimethyl-5-phenyltetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C

3.1: aluminium(III) triflate / dichloromethane / 10 h / Reflux

With lithium aluminium tetrahydride; aluminium(III) triflate; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/om401070c

Reference yield:

: 870-63-3
prenyl bromide

: 1512853-94-9
rac-2,2,5-trimethyl-5-phenyltetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C

3.1: aluminium(III) triflate / dichloromethane / 10 h / Reflux

With lithium aluminium tetrahydride; aluminium(III) triflate; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/om401070c