1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol

Base Information

Chemical Name:1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol
CAS No.:82994-35-2
Molecular Formula:C₂₄H₂₄O₃
Molecular Weight:360.453
Hs Code.:

Synonyms:

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Chemical Property of 1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol

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Technology Process of 1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol

There total 11 articles about 1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 499-75-2
carvacrol

: 82994-35-2
1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol

Guidance literature:: Multi-step reaction with 11 steps

1: 1.) DMAP, 2.) AlCl₃ / 1.) CHCl₃, reflux, 2.5 h, 2.) 1,2-dichloroethane, room temperature, 10 min

2: LiAlH₄ / diethyl ether / 0.17 h / Heating

3: 5.2 g / K₅IO₆, aq. H₂SO₄ / ethanol / 1.) 0 deg C, 2 h, 2.) 0 deg C to room temperature

4: 9.5 g / K₂CO₃ / acetone / 3 h / Heating

5: LiCl / H₂O; dimethylsulfoxide / 2 h / 165 °C

6: LiAlH₄ / diethyl ether / 2 h / Heating

7: MnO₂ / benzene / 12 h / Heating

8: tetrahydrofuran / 20 h / Ambient temperature

9: 0.5 h / Heating

10: 2.9 g / LiAlH₄ / tetrahydrofuran / 2 h / Heating

11: 5.2 g / K₂CO₃ / acetone / 2.5 h / Heating

With dmap; manganese(IV) oxide; lithium aluminium tetrahydride; aluminium trichloride; K₅IO₆; sulfuric acid; potassium carbonate; lithium chloride; In tetrahydrofuran; diethyl ether; ethanol; water; dimethyl sulfoxide; acetone; benzene;

Reference yield:

: 1665-99-2
2-hydroxy-6-isopropyl-3-methyl-benzaldehyde

: 82994-35-2
1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol

Guidance literature:: Multi-step reaction with 8 steps

1: 9.5 g / K₂CO₃ / acetone / 3 h / Heating

2: LiCl / H₂O; dimethylsulfoxide / 2 h / 165 °C

3: LiAlH₄ / diethyl ether / 2 h / Heating

4: MnO₂ / benzene / 12 h / Heating

5: tetrahydrofuran / 20 h / Ambient temperature

6: 0.5 h / Heating

7: 2.9 g / LiAlH₄ / tetrahydrofuran / 2 h / Heating

8: 5.2 g / K₂CO₃ / acetone / 2.5 h / Heating

With manganese(IV) oxide; lithium aluminium tetrahydride; potassium carbonate; lithium chloride; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide; acetone; benzene;

Reference yield:

: 82994-31-8
4-isopropyl-7-methyl-2-benzofurancarboxaldehyde

: 82994-35-2
1-benzyloxy-9-isopropyl-6-methyldibenzofuran-3-ylmethanol

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 20 h / Ambient temperature

2: 0.5 h / Heating

3: 2.9 g / LiAlH₄ / tetrahydrofuran / 2 h / Heating

4: 5.2 g / K₂CO₃ / acetone / 2.5 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;