XMD-12-3-1

Base Information

Chemical Name:XMD-12-3-1
CAS No.:1234481-10-7
Molecular Formula:C₂₀H₂₀N₆O₃S
Molecular Weight:424.483
Hs Code.:

Synonyms:

Suppliers and Price of XMD-12-3-1

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of XMD-12-3-1

Chemical Property:

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Technology Process of XMD-12-3-1

There total 3 articles about XMD-12-3-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1234479-75-4
2-chloro-5,11-dimethyl-5,11-dihydro-6H-benzo[e]pyrimido[5,4-b][1,4]diazepin-6-one

: 53297-70-4
4-amino-3-methylbenzenesulfonamide

: 1234481-10-7
XMD-12-3-1

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; XPhos; In 1,4-dioxane; at 95 ℃;
DOI:10.1021/acsmedchemlett.6b00209

Reference yield:

: 78726-75-7
3-methyl-4-nitrobenzene-1-sulfonyl chloride

: 1234481-10-7
XMD-12-3-1

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia; triethylamine / dichloromethane / 20 °C

2: hydrogen; palladium on activated charcoal / methanol / 20 °C

3: XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate / 1,4-dioxane / 95 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium on activated charcoal; ammonia; hydrogen; caesium carbonate; triethylamine; XPhos; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/acsmedchemlett.6b00209

Reference yield:

: 66427-86-9
2-chloro-11-methyl-5,11-dihydro-6H-benzo[e]pyrimido-[5,4-b][1,4]diazepin-6-one

: 1234481-10-7
XMD-12-3-1

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 °C

2: XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate / 1,4-dioxane / 95 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; caesium carbonate; XPhos; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.6b00209