Bromphosphan

Base Information

Chemical Name:Bromphosphan
CAS No.:150295-86-6
Molecular Formula:C₁₀H₁₄BrPSi
Molecular Weight:273.184
Hs Code.:

Brom<phenyl(trimethylsilyl)methylen>phosphan

Synonyms:

Suppliers and Price of Bromphosphan

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bromphosphan

Chemical Property:

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Technology Process of Bromphosphan

There total 1 articles about Bromphosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 82101-78-8
C₁₀H₁₅Br₂PSi

: 82101-81-3,150295-86-6
Bromphosphan

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In diethyl ether;
DOI:10.1016/S0040-4039(01)92391-3

Reference yield: 87.0%

: 82101-81-3,150295-86-6
Bromphosphan

: 109-89-7
diethylamine

: 138983-15-0
(Diethylamino)phosphan

Guidance literature:: With triethylamine; In pentane; for 12h; Ambient temperature;

Reference yield: 85.0%

: 12126-18-0
(η(5)-cyclopentadienyl)tricarbonylmolybdate

: 82101-81-3,150295-86-6
Bromphosphan

: tricarbonyl(η5-cyclopentadienyl){phenyl(trimethylsilyl)methylenephosphanyl}molybdenum

Guidance literature:: In tetrahydrofuran; addn. of phosphaalkene to soln. of alkali Mo complex under inert gas at -50°C; stirring, -50°C, 1h; warming to room temp.; stirring, 2h; evapn. of solvent, dissoln. in pentane, filtn., crystn. at -25°C, elem. anal.;