Technology Process of C19H24F4N4O9
There total 5 articles about C19H24F4N4O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 0 - 20 °C
2: methanol; sodium methylate / 1 h / 20 °C
3: palladium on carbon; hydrogen / methanol / 1 h / 20 °C
4: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere
With
methanol; palladium on carbon; boron trifluoride diethyl etherate; hydrogen; sodium methylate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05040k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium azide / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 24 h / 0 - 20 °C
3: methanol; sodium methylate / 1 h / 20 °C
4: palladium on carbon; hydrogen / methanol / 1 h / 20 °C
5: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere
With
methanol; sodium azide; palladium on carbon; boron trifluoride diethyl etherate; hydrogen; sodium methylate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05040k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on carbon; hydrogen / methanol / 1 h / 20 °C
2: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere
With
palladium on carbon; hydrogen;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05040k